Handbook of GC-MS: Fundamentals and Applications

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9783527334742: Handbook of GC-MS: Fundamentals and Applications

The only comprehensive reference on this popular and rapidly developing technique provides a detailed overview, ranging from fundamentals to applications, including a section on the evaluation of GC-MS analyses.
As such, it covers all aspects, including the theory and principles, as well as a broad range of real-life examples taken from laboratories in environmental, food, pharmaceutical and clinical analysis. It also features a glossary of approximately 300 terms and a substance index that facilitates finding a specific application.
For this new edition the work has been now extended to two volumes, reflecting the latest developments in the technique and related instrumentation, while also incorporating several new examples of applications in many fields.
The first two editions were very well received, making this handbook a must-have in all analytical laboratories using GC-MS.

Les informations fournies dans la section « Synopsis » peuvent faire référence à une autre édition de ce titre.

From the Back Cover :

Nowadays, gas chromatography/mass spectrometry is a frequently-used technique, with applications in food, pharmaceutical, clinical and environmental analysis. It allows both the separation of mixtures and the identification of the individual compounds of a mixture in one instrument.
This is the only comprehensive reference on the technique, providing a detailed overview ranging from fundamentals to applications. As such, it covers all aspects, including the theory and principles, as well as a broad range of real-life examples taken from laboratories. It also features a glossary of approximately 300 terms and a substance index that facilitates finding a specific application.
For this new edition the handbook has been now extended to two volumes, reflecting the latest developments in the technique and related instrumentation.
A must-have in all analytical laboratories using GC-MS.

About the Author :

Hans-Joachim Huebschmann graduated as Certified Food Chemist from the Technical University in Berlin, Germany, working in the field of LC-MS residue analysis of anabolic agents and pesticides in food. He started his career in diagnostics and medical analytical instruments before working for a number of German companies in gas chromatography and mass spectrometry. In 2002 he joined Thermo Fisher Scientific in Bremen, Germany, and held different international positions including Channel Manager for inorganic and isotope ratio mass spectrometry, Product Manager for high resolution GC-MS and GC-MS/MS, setting up the well-known POPs Center of Excellence in Bremen, Germany. From his role as the Technology Manager for GC-MS in Austin, Texas, USA, he moved to Thermo Asia operations in Singapore as the Technology Director for GC & GC-MS. Hans very recently joined CTC Analytics AG, a privately owned Swiss company, supporting and developing front-end automation in gas and liquid chromatography for innovative sample preparation solutions.

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Description du livre État : New. Publisher/Verlag: Wiley-VCH | Fundamentals and Applications | This new edition of the only comprehensive reference on GC-MS provides a detailed overview, including a wide range of real-life examples taken from clinical analysis. Now extended to two volumes, reflecting the latest developments in the technique and related instrumentation. | The only comprehensive reference on this popular and rapidly developing technique provides a detailed overview, ranging from fundamentals to applications, including a section on the evaluation of GC-MS analyses.As such, it covers all aspects, including the theory and principles, as well as a broad range of real-life examples taken from laboratories in environmental, food, pharmaceutical and clinical analysis. It also features a glossary of approximately 300 terms and a substance index that facilitates finding a specific application.For this new edition the work has been now extended to two volumes, reflecting the latest developments in the technique and related instrumentation, while also incorporating several new examples of applications in many fields.The first two editions were very well received, making this handbook a must-have in all analytical laboratories using GC-MS. | Foreword XIIIPreface to the Third Edition XV1 Introduction 11.1 The Historical Development of the GC-MS Technique 42 Fundamentals 72.1 Sample Preparation 72.1.1 Solid Phase Extraction 82.1.2 Solid Phase Microextraction 142.1.3 Pressurized Liquid Extraction 192.1.3.1 In-Cell Sample Preparation 232.1.3.2 In-Cell Moisture Removal 232.1.3.3 In-Cell Hydrocarbon Oxidation 242.1.4 Online Liquid Chromatography Clean-Up 252.1.5 Headspace Techniques 262.1.5.1 Static Headspace Technique 272.1.5.2 Dynamic Headspace Technique (Purge and Trap) 372.1.5.3 Coupling of Purge and Trap with GC-MS Systems 502.1.5.4 Headspace versus Purge and Trap 512.1.6 Adsorptive Enrichment and Thermal Desorption 572.1.6.1 Sample Collection 612.1.6.2 Calibration 622.1.6.3 Desorption 652.1.7 Pyrolysis 682.1.7.1 Foil Pyrolysis 702.1.7.2 Curie Point Pyrolysis 722.1.7.3 Micro-furnace Pyrolysis 752.1.8 Thermal Extraction (Outgassing) 762.1.9 QuEChERS Sample Preparation 792.2 Gas Chromatography 852.2.1 Sample Inlet Systems 852.2.2 Carrier Gas Regulation 872.2.2.1 Forward Pressure Regulation 872.2.2.2 Back Pressure Regulation 882.2.2.3 Carrier Gas Saving 892.2.3 Injection Port Septa 912.2.3.1 Septum Purge 932.2.3.2 The MicroSeal Septum 932.2.4 Injection Port Liner 952.2.4.1 Split Injection 952.2.4.2 Splitless Injection 962.2.4.3 Liner Activity and Deactivation 962.2.4.4 Liner Geometry 982.2.5 Vaporizing Sample Injection Techniques 992.2.5.1 Hot Needle Thermo Spray Injection Technique 1002.2.5.2 Cold Needle Liquid Band Injection Technique 1022.2.5.3 Filled Needle Injections 1032.2.5.4 Split Injection 1042.2.5.5 Splitless Injection (Total Sample Transfer) 1042.2.5.6 Concurrent Solvent Recondensation 1072.2.5.7 Concurrent Backflush 1082.2.6 Temperature Programmable Injection Systems 1142.2.6.1 The PTV Cold Injection System 1152.2.6.2 The PTV Injection Procedures 1172.2.6.3 On-Column Injection 1242.2.6.4 PTV On-Column Injection 1272.2.6.5 Cryofocussing 1282.2.6.6 PTV Cryo-Enrichment 1292.2.7 Capillary Column Choice and Separation Optimization 1302.2.7.1 Sample Capacity 1392.2.7.2 Internal Diameter 1402.2.7.3 Film Thickness 1412.2.7.4 Column Length 1432.2.7.5 Setting the Carrier Gas Flow 1442.2.7.6 Properties of Column Phases 1452.2.7.7 Properties of Ionic Liquid Phases 1502.2.8 Chromatography Parameters 1532.2.8.1 The Chromatogram and Its Meaning 1552.2.8.2 Capacity Factor k 1562.2.8.3 Chromatographic Resolution 1572.2.8.4 Factors Affecting the Resolution 1592.2.8.5 Maximum Sample Capacity 1632.2.8.6 Peak Symmetry 1642.2.8.7 Optimization of Carrier Gas Flow 1642.2.8.8 Effect of Oven Temperature Ramp Rate 1682.2.9 Fast Gas Chromatography Solutions 1692.2.9.1 Fast Chromatography 1712.2.9.2 Ultra-Fast Chromatography 1752.2.10 Multi-Dimensional Gas Chromatography 1782. N° de réf. du libraire K9783527334742

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