High Resolution Nmr in the Solid State: Fundamentals of CP/Mas - Couverture rigide

Stejskal; Memory

Couverture rigide

ISBN 10 : 0195073800 ISBN 13 : 9780195073805

Editeur : Oxford University Press Inc, 1994

Synopsis

This text was developed from a course for physical chemistry and chemical physics students using cross-polarization (CP) magic angle spinning (MAS) NMR in their laboratory assignments. The book provides students with the details of the CP/MAS experiment as it is used to obtain rare-spin, high-resolution NMR spectra. The design of the CP/MAS experiments and the interpretation of spectra and relaxation measurements require an understanding of the interplay of several fundamental physical interactions not normally encountered in solution NMR. The student can observe the way interacting spin systems behave in the solid state, and have a quantum mechanically rigorous understanding of solid-state spin phenomena. The text will have the added benefit of serving as a self-study resource for students seeking to learn the underlying principles of laboratory experiments using the technique. The history of NMR is also treated, and the instrumentation of the spectrometer and probe are discussed.

A propos du livre

Présentation de l'éditeur

Nuclear Magnetic Resonance is used by both physicists and chemists to determine the structure and behaviour of solid materials. This book, for advanced undergraduates and graduate students in both disciplines, aims to provide substantial information on a particular spectroscopic experiment, the cross-polarization (CP) magic angle spinning (MAS) experiment, which is used to obtain rare-spin, high resolution NMR spectra. The text explains clearly the underlying principles of NMR, as well as those involved in this particular experimental method. It can be used by either the student or the working spectroscopist needing to learn the underlying principles of the laboratory experiments they are using.

Revue de presse

To say that the appearance of a book on the fundamentals of CP/MAS is timely would be a gross understatement ... this is an excellent book and should be read carefully, and understood, by all practitioners of CP/MAS NMT spectroscopy. (Glenn Penner, University of Guelph, Magnetic Resonance in Chemistry, Vol. 33 989 (1995))

Détails de l'édition

• Éditeur: Oxford University Press Inc
• Date d'édition: 1994
• Langue: anglais
• ISBN 10: 0195073800
• ISBN 13: 9780195073805
• Reliure: Relié
• Nombre de pages: 208
• Coordonnées du fabricant: non disponible
• Personne responsable: Ufficio Anagrafiche Messaggerie; ufficio.anagrafiche@meli.it; ; Via Verdi, 8; Assago Milano; 20090; Italie