Organic Structures from Spectra - Couverture souple

Sternhell, S.; Kalman, J. R.; Field, L.D.

Couverture souple

ISBN 10 : 0471956317 ISBN 13 : 9780471956310

Editeur : John Wiley & Sons Ltd, 2002

Synopsis

The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all universities. A critical part of any such course is a suitable set of problems to develop the student's understanding of how structures are derived. This book combines the subject matter of a minimal course needed to understand the major spectroscopic techniques with a carefully selected set of 181 structural problems involving the use of all the major techniques and 19 problems specifically dealing with the interpretation of spin-spin coupling in proton NMR spectra. The problems are graded to develop and consolidate the student's understanding of organic spectroscopy. The accompanying text indicates the level of theory required to tackle the problems. The examples themselves have been carefully selected to include all important structural features and to emphasise connectivity arguments. Many of the compounds were synthesised specifically for this purpose. There are many easier problems than in other collections. Strenuous efforts have been made to ensure that solutions to the 181 structural problems are unambiguous. The second edition of this popular and successful work has been significantly revised and updated, and contains some 70 additional carefully chosen problems. Most problems feature NMR spectra obtained at higher fields than in the first edition and DEPT experiments as well as coupled 13 C NMR spectra are included. Five problems are presented in the style of experimental sections of research papers and the Appendix contains two fully worked solutions. Contents include: Preface; Introduction; Ultraviolet Spectroscopy; Infrared Spectroscopy; Mass Spectrometry; Nuclear Magnetic Resonance Spectroscopy; Miscellaneous Topics; Problems; Appendix; and, Index.

A propos du livre

Quatrième de couverture

The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. A critical part of any such course is a suitable set of problems to develop the student s understanding of how structures are determined from spectra.

Organic Structures from Spectra, FourthEditionis a carefully chosen set of more than 280 structural problems employing the major modern spectroscopic techniques, a selection of 18 problems using 2D–NMR spectroscopy, more than 20 problems specifically dealing with the interpretation of spin–spin coupling in proton NMR spectra and 8 problems based on the quantitative analysis of mixtures using proton and carbon NMR spectroscopy. All of the problems are graded to develop and consolidate the student s understanding of organic spectroscopy. The accompanying text is descriptive and only explains the underlying theory at a level which is sufficient to tackle the problems. The text includes condensed tables of characteristic spectral properties covering the frequently encountered functional groups.

The examples themselves have been selected to include all important structural features and to emphasise connectivity arguments. Many of the compounds were synthesised specifically for this purpose. There are many more easy problems, to build confidence and demonstrate basic principles, than in other collections. 

The fourth edition of this popular textbook:

• now incorporates a suite of new problems dealing with the analysis of 2D NMR spectra (COSY, NOESY, TOCSY and C H Correlation spectroscopy);
• has been expanded and updated to reflect the new developments in the area;
• has an additional 25 carefully selected basic problems;
• provides a set of problems dealing specifically with the quantitative analysis of mixtures using NMR spectroscopy;
• features proton NMR spectra obtained at 200, 400 and 600 MHz and 13C NMR spectra include DEPT experiments as well as proton–coupled experiments;
• conatins 6 problems in the style of the experimental section of a research paper and the appendix contains examples of fully worked solutions.

Organic Structures from Spectra, Fourth Edition will prove invaluable for students of Chemistry, Pharmacy and Biochemistry taking a first course in Organic Chemistry.

Review from earlier edition

" I would definitely state that this book is the most useful aid to basic organic spectroscopy teaching in existence and I would strongly recommend every instructor in this area to use it either as a source of examples or as a class textbook."
Magnetic Resonance in Chemistry

Quatrième de couverture

The derivation of structural information from spectroscopic data is now an integral part of organic chemistry at all universities. A critical part of any such course is a suitable set of problems to develop the student′s understanding of how structures are derived.

Organic Structures for Spectra, Third Edition consists of a carefully selected set of 256 structural problems involving the use of all the major spectroscopic techniques and 20 problems that deal specifically with the interpretation of spin–spin coupling in proton NMR spectra. The problems are graded to develop and consolidate the student′s undestanding of Organic Spectroscopy. The accompanying text is descriptive and explains the underlying theory at a level that is appropriate for tackling the problems. The text includes condensed tables of characteristic spectral properties covering the frequently encountered functional groups.

The examples themselves have been carefully selected to include all–important structural features and to emphasise connectivity arguments. Many of the compounds were synthesised specifically for this purpose. There are many more easy problems (to build confidence and demonstrate basic principles) than in other collections. Strenuous efforts have been made to ensure that each of the structural problems has an unambiguous solution

The third edition of this popular textbook:
∗ has been expanded and updated to reflect the new developments in the area

∗ contains an additional 70 carefully chosen problems

∗ features NMR spectra obtaines at 200, 400 and 600 MHz and includes a selection of DEPT experiments as well as coupled ¯13C NMR spectra.

∗ includes 6 problems which are presented in the style of experimental sections of research papers and the appendix contains examples of fully worked solutions
Organic Structures from Spectra, Third Edition will prove invaluable for students of Chemistry, Pharmacy and Biochemistry taking a first course in Organic Chemistry.

Détails de l'édition

• Éditeur: John Wiley & Sons Ltd
• Date d'édition: 2002
• Langue: anglais
• ISBN 10: 0471956317
• ISBN 13: 9780471956310
• Reliure: Broché
• Numéro d'édition: 2
• Nombre de pages: 220
• Coordonnées du fabricant: non disponible