In Situ Raman Microscopy of a Single Graphite Microflake Electrode in a Li(+)-Containing Electrolyte - Couverture souple

 
9781289290818: In Situ Raman Microscopy of a Single Graphite Microflake Electrode in a Li(+)-Containing Electrolyte
Couverture souple
ISBN 10 : 1289290814 ISBN 13 : 9781289290818
Editeur : Bibliogov, 2013

Synopsis


Highly detailed Raman spectra from a single KS-44 graphite microflake electrode as a function of the applied potential have been collected in situ using a Raman microscope and a sealed spectroelectrochemical cell isolated from the laboratory environment. Correlations were found between the Raman spectral features and the various Li(+) intercalation stages while recording in real time Raman spectra during a linear potential scan from 0.7 down ca. 0.0V vs Li/Li(+) at a rate of 0.1 mV/s in a 1M LiClO4 solution in a 1: l (by volume) ethylene carbonate (EC): diethyl carbonate (DEC) mixture. In particular, clearly defined isosbestic points were observed for data collected in the potential range where the transition between dilute phase 1 and phase 4 of lithiated graphite is known to occur, i.e. 0.157

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Éditeur
Bibliogov
Date d'édition
2013
Langue
anglais
ISBN 10 
1289290814
ISBN 13 
9781289290818
Reliure
Broché
Nombre de pages
24
Coordonnées du fabricant
non disponible
Personne responsable
non disponible