The digital edition of all books may be viewed on our website before purchase. Excerpt from Methods in Chemical Analysis, Originated or Developed in the Kent Chemical Laboratory of Yale University (Classic Reprint)
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The tubes A and Bare so selected that very little of the product evolved can escape between them, and, in case they fit very loosely, a ring of paraffin melted into the mouth of A, about B, by means of a hot wire, seals the joint securely. A very convenient way to attach the paraffin is to melt it between A and another tube, which fits A, as does B, and may be removed by a turning motion, leaving the ring into which Bwill fit. Very little heating is then required to make a tight joint. If care be used in taking apart A and B, at the close of an experiment, such a ring of paraffin remains in place and may be used many times without replacement, being remelted by a touch of the hot wire before every new experiment. In making a determination, the substance under examination is weighed and placed in the bottom of A. The reagent to be employed, 10 cm.3 to 15 cm.3, is drawn into C, and held there in the manner described. The test tube A is slipped over B, and the joint is sealed with paraffin, as has been shown. The apparatus is wiped, placed on the balance and weighed. Upon removing the cap from the small tube in C, the reagent runs from Cinto A. The volatile product, forced upward through the drying column of calcium chloride, escapes through the annular space between Band C. When action ceases, a current of dry air is forced through C, to remove all the volatile product, the cap is replaced, and the apparatus is weighed. The loss of weight represents the volatile product. Hydrogen by Loss.
(Typographical errors above are due to OCR software and don't occur in the book.)
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Vendeur : Forgotten Books, London, Royaume-Uni
Paperback. Etat : New. Print on Demand. This book is a compendium of techniques developed at Yale University's Kent Chemical Laboratory for the analysis of chemical substances. It provides detailed, concise procedures for measuring substances that exist as gases at room temperature, distilling and condensing volatile products, and removing volatile products without losing non-volatile material. The book also describes methods for preventing mechanical loss from solution in reactions evolving gaseous products, transferring liquids and gases under pressure, purifying precipitates by solution and reprecipitation, and using electrolytic processes. The author has adapted and improved upon existing procedures, and has developed new methods to meet specific challenges encountered in the laboratory. By presenting these methods in a clear and accessible format, the author aims to empower chemists with the tools they need to conduct accurate and efficient analyses. This book is a reproduction of an important historical work, digitally reconstructed using state-of-the-art technology to preserve the original format. In rare cases, an imperfection in the original, such as a blemish or missing page, may be replicated in the book. print-on-demand item. N° de réf. du vendeur 9781330663288_0
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Vendeur : PBShop.store US, Wood Dale, IL, Etats-Unis
PAP. Etat : New. New Book. Shipped from UK. Established seller since 2000. N° de réf. du vendeur LW-9781330663288
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Vendeur : PBShop.store UK, Fairford, GLOS, Royaume-Uni
PAP. Etat : New. New Book. Shipped from UK. Established seller since 2000. N° de réf. du vendeur LW-9781330663288
Quantité disponible : 15 disponible(s)