100 and More Basic NMR Experiments: A Practical Course - Couverture souple

Braun, Siegmar; Etc.; Kalinowski, H.-O.; Berger, S.

Couverture souple

ISBN 10 : 3527290915 ISBN 13 : 9783527290918

Editeur : Wiley-VCH Verlag GmbH, 1996

Synopsis

This practical course aims to enable the reader to understand the field of NMR experiments for structure determination. The experiments featured have been chosen mainly because of their importance and general applicability. Three compounds have been chosen as the main demonstration samples - chloroform, ethyl crotonate and strychnine (which should be used as a sealed sample). A scheme has been adopted for the detailed description of the experiments, organized in the following specific sections: "Purpose" explains the idea and goal of the experiment and refers the user to related experiments; "Literature" presents references to the original publication and to improvements and/or sections in monographs and reviews; "Pulse Scheme and Phase Cycle" gives the pulse sequence in an instrument-independent graphic and self-explanatory form, and the phase cycles of the pulses and the receiver; "Acquisition" is the main section, with instructions on the sample to be used, the spectrometer configuration, the type of programme and the parameters necessary for the performance of the experiment; "Processing" describes how to treat the time-domain data; "Results" presents the spectrum obtained by following the procedure exactly; and "Comments" contains an explanation of the most important steps of the pulse sequence. In general, the conditions for the experiments have not been optimized. In all cases, the results are presented exactly as they were obtained, without cosmetic retouching; sometimes, the samples used even show impurities.

A propos du livre

Revue de presse

... an essential purchase for all NMR devotees ... honest, well focused and most adequately produced ... A wealth of information is clearly expressed and provided. Post–graduate students will find it of particular value.
Analyst

.. it is a marvelous and magnificent teaching book as well for beginners as for masters having to teach NMR. We like enormousy such manner to consider the learning of a new technique and we hope that many, if not all our readers will follow this new "Champs Elysées" or "Campus Elisearum", the pathway followed by gods in the greek mythology, but having become the daily highway of the scientists, who are, in some part, the followers of these gods, since they create all new stuff for the progress of the science.
Cellular and Molecular Biology

Présentation de l'éditeur

How do the pulse sequences of modern NMR work? Which experiment conveys the desired information? How can the maximal amount of information be retrieved from measured spectra?

Have you ever been confronted with questions like these?

Get the answers and explore the full productivity of your NMR equipment! This book is a reliable guide through the maze of modern NMR tools. Written by leading experts, it describes more than a hundred NMR experiments including selective pulses, field gradients and the second and third dimension.

Being textbook as well as reference book for the laboratory, this book is a must for every scientist working with NMR as well as for students preparing for their lab courses.

Détails de l'édition

• Éditeur: Wiley-VCH Verlag GmbH
• Date d'édition: 1996
• Langue: anglais
• ISBN 10: 3527290915
• ISBN 13: 9783527290918
• Reliure: Broché
• Nombre de pages: 430
• Coordonnées du fabricant: non disponible
• Personne responsable: non disponible