Articles liés à Transition metal complexes of thiosemicarbazone: Study...

Transition metal complexes of thiosemicarbazone: Study of Cu(II), Ni(II)and Co(II) complexes of thiosemicarbezide attached with quinoline aldehydes - Couverture souple

Tada, Rakesh; Nakum, Kiran; Chavda, Naimish

 
9783844322316: Transition metal complexes of thiosemicarbazone: Study of Cu(II), Ni(II)and Co(II) complexes of thiosemicarbezide attached with quinoline aldehydes
Couverture souple
ISBN 10 : 3844322310 ISBN 13 : 9783844322316
Editeur : LAP LAMBERT Academic Publishing, 2014

Synopsis

Summarizes the preparation and structure characterization of various thiosemicarbazones attached Quinoline aldehyde as well as their metal complexes. Synthesized ligands and metal complexes were characterized by different technique like mass, IR, 1H NMR, 13C NMR, UV-Visible spectroscopy as well as elemental analysis. In the elemental analysis of the synthesized compound both calculated and found percentages of elements are matched so elemental analysis confirms the structure of the thiosemicarbazone. Mass spectral data confirm the structure of the ligand as indicated by the molecular ion peak (M+) corresponding to their molecular weight. In IR spectra of the synthesized thiosemicarbazone showed useful information about the structure of the compound. In the IR spectra, some significant stretching bands due to -N-H, -N-N-, -NH2 and -C=S were observed at specific frequencies. In the 1H NMR spectra, the signal due to -CH=N-, -N-NH, NH2 and aromatic protons were observed in the expected regions. The 13C NMR spectrum provides direct information about the carbon skeleton of the synthesized compound.

Les informations fournies dans la section « Synopsis » peuvent faire référence à une autre édition de ce titre.

Présentation de l'éditeur

Summarizes the preparation and structure characterization of various thiosemicarbazones attached Quinoline aldehyde as well as their metal complexes. Synthesized ligands and metal complexes were characterized by different technique like mass, IR, 1H NMR, 13C NMR, UV-Visible spectroscopy as well as elemental analysis. In the elemental analysis of the synthesized compound both calculated and found percentages of elements are matched so elemental analysis confirms the structure of the thiosemicarbazone. Mass spectral data confirm the structure of the ligand as indicated by the molecular ion peak (M+) corresponding to their molecular weight. In IR spectra of the synthesized thiosemicarbazone showed useful information about the structure of the compound. In the IR spectra, some significant stretching bands due to -N-H, -N-N-, -NH2 and -C=S were observed at specific frequencies. In the 1H NMR spectra, the signal due to -CH=N-, -N-NH, NH2 and aromatic protons were observed in the expected regions. The 13C NMR spectrum provides direct information about the carbon skeleton of the synthesized compound.

Biographie de l'auteur

Department of chemistryd.k.v.arts & science college-jamnagar(gujarat)

Les informations fournies dans la section « A propos du livre » peuvent faire référence à une autre édition de ce titre.

Éditeur
LAP LAMBERT Academic Publishing
Date d'édition
2014
Langue
anglais
ISBN 10 
3844322310
ISBN 13 
9783844322316
Reliure
Broché
Nombre de pages
68
Coordonnées du fabricant
non disponible
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