Preparation of Oxadiazole Complexes: Preparation and Characterization of Oxadiazole and Hydrazino Benzothiazole and Their Transition Metal Complexes - Couverture souple

Yousif, Emad; Ahmed, Hamsa; Jassim, Ayad

Couverture souple

ISBN 10 : 3848427850 ISBN 13 : 9783848427857

Editeur : LAP LAMBERT Academic Publishing, 2012

A propos du livre

Présentation de l'éditeur

Three new ligands have been prepared in this work, which were chosen to synthesis a new set of transition metal complexes [Cu (II), Ni (II), Hg (II), Cd (II) and Co (II)]. LI=(2-[5-phenyl-2-methylthio-1,3,4-oxadizole]-5-phenyl-1,3,4-oxadiazole), LII=2-(O-chloro benzylidine) hydrazine benzothiazole and LIII=2-(p-hydroxy benzylidine) hydrazine benzothiazole were prepared by Schiff reaction between 2-mercaptobenzothiazole and 2-chlorobenzaldehyde and p-hydroxy benzaldehyde. The new ligands were characterized by the Infra-red spectroscopy and melting points. The metal complexes, were prepared and isolated in pure solid state, and found to be stable toward light, heat and moisture. These new complexes were characterized via FT.IR , UV-Vis Spectroscopy, magnetic and conductivity measurements. In addition the metal contain were determind by atomic absorption measurement. Different bonding and structural behavior were revealed through the study of the coordination chemistry of the metal complexes of the new ligands.

Biographie de l'auteur

Hamsa Ahmed and Ayad Jassim:Department of Chemistry, College of Science, Al-Nahrain University, Baghdad, Iraq

Détails de l'édition

• Éditeur: LAP LAMBERT Academic Publishing
• Date d'édition: 2012
• Langue: anglais
• ISBN 10: 3848427850
• ISBN 13: 9783848427857
• Reliure: Broché
• Nombre de pages: 92
• Coordonnées du fabricant: non disponible
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