Development of RP-HPLC, HPTLC and UV-Visible Spectrophotometry Methods - Couverture souple

Khan, Zamir G ; Shirkhedkar, Atul A

9786139847150: Development of RP-HPLC, HPTLC and UV-Visible Spectrophotometry Methods

Couverture souple

ISBN 10 : 613984715X ISBN 13 : 9786139847150

Editeur : LAP Lambert Academic Publishing, 2018

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�diteur: LAP Lambert Academic Publishing
Date d'�dition: 2018
Langue: anglais
ISBN 10: 613984715X
ISBN 13: 9786139847150
Reliure: Broch�
Nombre de pages: 104
Coordonn�es du fabricant: non disponible
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Development of RP-HPLC, HPTLC and UV-Visible Spectrophotometry Methods

Zamir G. Khan

Edit� par LAP LAMBERT Academic Publishing Mai 2018, 2018

ISBN 10 : 613984715X ISBN 13 : 9786139847150

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Taschenbuch. Etat : Neu. This item is printed on demand - it takes 3-4 days longer - Neuware -Six methods RP-HPLC, RP-HPTLC/densitometry and UV-Spectrophotometry (first order amplitude, first order AUC, second-order amplitude and second order AUC) have been developed for the determination of tadalafil in bulk and pharmaceutical formulation. RP-HPLC and RP-HPTLC/Densitometry methods are found to be accurate, precise, rugged and robust. Both these methods are adequately sensitive. The only limitation of RP-HPLC and RP-HPTLC/densitometry method is their cost. For RP-HPLC study, Design Expert software ver. 8.0.4 was used to study robustness parameter, which showed that method is robust. From results of ANOVA and analysis of response surfaces plots; it can be concluded that responses, y1 (Retention time) and y2 (Tailing factor) are robust for x1, x2, and x3; however, for y3(Theoretical plates) x1, x2, and x3 affect considerably. All four UV-Spectrophotometric methods are simple, accurate, precise and least calculations are involved for estimation of concentrations of the drug. No interference of the excipients was observed in any one of the methods during tablet assay. All the developed methods can be used for routine analysis of tadalafil in the pharmaceutical formulation. 104 pp. Englisch. N� de r�f. du vendeur 9786139847150

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Development of RP-HPLC, HPTLC and UV-Visible Spectrophotometry Methods

Zamir G Khan

Edit� par LAP Lambert Academic Publishing, 2018

ISBN 10 : 613984715X ISBN 13 : 9786139847150

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Development of RP-HPLC, HPTLC and UV-Visible Spectrophotometry Methods

Zamir G Khan

Edit� par LAP Lambert Academic Publishing, 2018

ISBN 10 : 613984715X ISBN 13 : 9786139847150

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Development of RP-HPLC, HPTLC and UV-Visible Spectrophotometry Methods

Zamir G. Khan|Atul A. Shirkhedkar

Edit� par LAP LAMBERT Academic Publishing, 2018

ISBN 10 : 613984715X ISBN 13 : 9786139847150

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Etat : New. Dieser Artikel ist ein Print on Demand Artikel und wird nach Ihrer Bestellung fuer Sie gedruckt. Autor/Autorin: Khan Zamir G.Mr. Zamir G Khan is working as Asst. Professor H. R. Patel Institute of Pharmaceutical Education & Research, Shirpur (M.S.) from 2014. He received his master degree in Pharmaceutical Chemistry in 2014 and Bachelor Degree. N� de r�f. du vendeur 385874113

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Development of RP-HPLC, HPTLC and UV-Visible Spectrophotometry Methods

Zamir G Khan

Edit� par LAP Lambert Academic Publishing, 2018

ISBN 10 : 613984715X ISBN 13 : 9786139847150

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Development of RP-HPLC, HPTLC and UV-Visible Spectrophotometry Methods

Atul A. Shirkhedkar

Edit� par LAP LAMBERT Academic Publishing, 2018

ISBN 10 : 613984715X ISBN 13 : 9786139847150

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Taschenbuch. Etat : Neu. nach der Bestellung gedruckt Neuware - Printed after ordering - Six methods RP-HPLC, RP-HPTLC/densitometry and UV-Spectrophotometry (first order amplitude, first order AUC, second-order amplitude and second order AUC) have been developed for the determination of tadalafil in bulk and pharmaceutical formulation. RP-HPLC and RP-HPTLC/Densitometry methods are found to be accurate, precise, rugged and robust. Both these methods are adequately sensitive. The only limitation of RP-HPLC and RP-HPTLC/densitometry method is their cost. For RP-HPLC study, Design Expert software ver. 8.0.4 was used to study robustness parameter, which showed that method is robust. From results of ANOVA and analysis of response surfaces plots; it can be concluded that responses, y1 (Retention time) and y2 (Tailing factor) are robust for x1, x2, and x3; however, for y3(Theoretical plates) x1, x2, and x3 affect considerably. All four UV-Spectrophotometric methods are simple, accurate, precise and least calculations are involved for estimation of concentrations of the drug. No interference of the excipients was observed in any one of the methods during tablet assay. All the developed methods can be used for routine analysis of tadalafil in the pharmaceutical formulation. N� de r�f. du vendeur 9786139847150

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Development of RP-HPLC, HPTLC and UV-Visible Spectrophotometry Methods

Zamir G. Khan

Edit� par LAP LAMBERT Academic Publishing Mai 2018, 2018

ISBN 10 : 613984715X ISBN 13 : 9786139847150

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Vendeur : buchversandmimpf2000, Emtmannsberg, BAYE, Allemagne

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Taschenbuch. Etat : Neu. This item is printed on demand - Print on Demand Titel. Neuware -Six methods RP-HPLC, RP-HPTLC/densitometry and UV-Spectrophotometry (first order amplitude, first order AUC, second-order amplitude and second order AUC) have been developed for the determination of tadalafil in bulk and pharmaceutical formulation. RP-HPLC and RP-HPTLC/Densitometry methods are found to be accurate, precise, rugged and robust. Both these methods are adequately sensitive. The only limitation of RP-HPLC and RP-HPTLC/densitometry method is their cost. For RP-HPLC study, Design Expert software ver. 8.0.4 was used to study robustness parameter, which showed that method is robust. From results of ANOVA and analysis of response surfaces plots; it can be concluded that responses, y1 (Retention time) and y2 (Tailing factor) are robust for x1, x2, and x3; however, for y3(Theoretical plates) x1, x2, and x3 affect considerably. All four UV-Spectrophotometric methods are simple, accurate, precise and least calculations are involved for estimation of concentrations of the drug. No interference of the excipients was observed in any one of the methods during tablet assay. All the developed methods can be used for routine analysis of tadalafil in the pharmaceutical formulation.VDM Verlag, Dudweiler Landstra�e 99, 66123 Saarbr�cken 104 pp. Englisch. N� de r�f. du vendeur 9786139847150

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Development of RP-HPLC, HPTLC and UV-Visible Spectrophotometry Methods

Zamir G. Khan (u. a.)

Edit� par LAP LAMBERT Academic Publishing, 2018

ISBN 10 : 613984715X ISBN 13 : 9786139847150

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