Stability-Indicating Chromatographic Methods - Couverture souple

Pethani, Trupesh ; Thumar, Mayuri ; Bavaliya, Paresh

9786208462345: Stability-Indicating Chromatographic Methods

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ISBN 10 : 6208462347 ISBN 13 : 9786208462345

Editeur : LAP Lambert Academic Publishing, 2025

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�diteur: LAP Lambert Academic Publishing
Date d'�dition: 2025
Langue: anglais
ISBN 10: 6208462347
ISBN 13: 9786208462345
Reliure: Broch�
Nombre de pages: 112
Coordonn�es du fabricant: non disponible
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Stability-Indicating Chromatographic Methods

Pethani, Trupesh; Thumar, Mayuri; Bavaliya, Paresh

Edit� par LAP LAMBERT Academic Publishing, 2025

ISBN 10 : 6208462347 ISBN 13 : 9786208462345

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Stability-Indicating Chromatographic Methods

Pethani, Trupesh; Thumar, Mayuri; Bavaliya, Paresh

Edit� par LAP LAMBERT Academic Publishing, 2025

ISBN 10 : 6208462347 ISBN 13 : 9786208462345

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Stability-Indicating Chromatographic Methods

Pethani, Trupesh; Thumar, Mayuri; Bavaliya, Paresh

Edit� par LAP Lambert Academic Publishing, 2025

ISBN 10 : 6208462347 ISBN 13 : 9786208462345

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STABILITY-INDICATING CHROMATOGRAPHIC METHODS

Trupesh Pethani

Edit� par LAP LAMBERT Academic Publishing Sep 2025, 2025

ISBN 10 : 6208462347 ISBN 13 : 9786208462345

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Taschenbuch. Etat : Neu. This item is printed on demand - it takes 3-4 days longer - Neuware 112 pp. Englisch. N� de r�f. du vendeur 9786208462345

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Stability-Indicating Chromatographic Methods (Paperback)

Trupesh Pethani

Edit� par LAP Lambert Academic Publishing, 2025

ISBN 10 : 6208462347 ISBN 13 : 9786208462345

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Paperback. Etat : new. Paperback. The present work focused on developing and validating simple, precise, accurate, sensitive, and stability-indicating chromatographic methods for the simultaneous estimation of Tolperisone Hydrochloride and Diclofenac Sodium in combined pharmaceutical dosage forms. Although RP-HPLC and HPTLC methods had been reported for their assay, no stability-indicating methods were available in literature. Hence, methods were developed as per ICH guidelines to ensure reliability in quality control. The optimized RP-HPLC method employed a Kromasil C18 column with methanol, acetonitrile, and water (80:16:4, pH 3.0) as mobile phase, showing retention times of 2.93 min for Tolperisone and 4.20 min for Diclofenac. The HPTLC method used silica gel 60 F254 plates with methanol: toluene: ethyl acetate (2.5:7:0.5 v/v/v), yielding Rf values of 0.5 and 0.7, respectively. Both methods were validated for linearity, precision, accuracy, robustness, LOD, and LOQ, with recoveries close to 99-100%. Forced degradation under acidic, alkaline, oxidative, thermal, and photolytic conditions confirmed method specificity, revealing Tolperisone to be more labile than Diclofenac. This item is printed on demand. Shipping may be from our UK warehouse or from our Australian or US warehouses, depending on stock availability. N� de r�f. du vendeur 9786208462345

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Stability-Indicating Chromatographic Methods

Pethani, Trupesh; Thumar, Mayuri; Bavaliya, Paresh

Edit� par LAP Lambert Academic Publishing, 2025

ISBN 10 : 6208462347 ISBN 13 : 9786208462345

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Stability-Indicating Chromatographic Methods

Pethani, Trupesh; Thumar, Mayuri; Bavaliya, Paresh

Edit� par LAP Lambert Academic Publishing, 2025

ISBN 10 : 6208462347 ISBN 13 : 9786208462345

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STABILITY-INDICATING CHROMATOGRAPHIC METHODS

Trupesh Pethani

Edit� par LAP LAMBERT Academic Publishing Sep 2025, 2025

ISBN 10 : 6208462347 ISBN 13 : 9786208462345

Neuf Taschenbuch

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Vendeur : buchversandmimpf2000, Emtmannsberg, BAYE, Allemagne

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Taschenbuch. Etat : Neu. This item is printed on demand - Print on Demand Titel. Neuware -The present work focused on developing and validating simple, precise, accurate, sensitive, and stability-indicating chromatographic methods for the simultaneous estimation of Tolperisone Hydrochloride and Diclofenac Sodium in combined pharmaceutical dosage forms. Although RP-HPLC and HPTLC methods had been reported for their assay, no stability-indicating methods were available in literature. Hence, methods were developed as per ICH guidelines to ensure reliability in quality control. The optimized RP-HPLC method employed a Kromasil C18 column with methanol, acetonitrile, and water (80:16:4, pH 3.0) as mobile phase, showing retention times of 2.93 min for Tolperisone and 4.20 min for Diclofenac. The HPTLC method used silica gel 60 F254 plates with methanol:toluene:ethyl acetate (2.5:7:0.5 v/v/v), yielding Rf values of 0.5 and 0.7, respectively. Both methods were validated for linearity, precision, accuracy, robustness, LOD, and LOQ, with recoveries close to 99-100%. Forced degradation under acidic, alkaline, oxidative, thermal, and photolytic conditions confirmed method specificity, revealing Tolperisone to be more labile than Diclofenac.VDM Verlag, Dudweiler Landstra�e 99, 66123 Saarbr�cken 112 pp. Englisch. N� de r�f. du vendeur 9786208462345

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