Fabrication of TiO2 Nanotubes Using Electrochemical Anodization: TiO2 Nanotubes - Couverture souple

Abdul Muhsien Hassan, Marwa; Al-Eqaby, Haidar H.Hamdan

 
9783659157721: Fabrication of TiO2 Nanotubes Using Electrochemical Anodization: TiO2 Nanotubes

Synopsis

In this work, describes the synthesis of self-organized titanium dioxide nanotube layers by an electrochemical anodization of Ti at different conditions (time, voltage, concentration of NH4F in electrolyte with glycerol, conductivity and water content) at room temperature (~25ºC) were investigated. In the current study, self-organized,vertically-oriented TiO2 nanotubes were successfully prepared by anodization method of a pure Titanium sheet (99.5%) using anodization cell is designed for first time in Iraq (Homemade) from Teflon material according to our knowledge to produce self-ordered Titanium nanotube in organic based electrolytes (glycerol based electrolyte) an electrolyte solution containing (0.5, 1, 1.5 and 2 wt.% NH4F) then added water (2 and 5Wt.% H2O) to (0.5wt.% NH4F) only with 15V. The range of anodizing time and potential were between 1-4hr. and 5-40V, where Wt.% represent weight percentage. Scanning electron microscopy (SEM), Atomic force microscopy (AFM) and (XRD) X-Ray diffraction were employed to characterize the morphology and structure of the obtained Titania templates, optical interferometer (Fizeau frings) method to tubes length measurement.

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Présentation de l'éditeur

In this work, describes the synthesis of self-organized titanium dioxide nanotube layers by an electrochemical anodization of Ti at different conditions (time, voltage, concentration of NH4F in electrolyte with glycerol, conductivity and water content) at room temperature (~25ºC) were investigated. In the current study, self-organized,vertically-oriented TiO2 nanotubes were successfully prepared by anodization method of a pure Titanium sheet (99.5%) using anodization cell is designed for first time in Iraq (Homemade) from Teflon material according to our knowledge to produce self-ordered Titanium nanotube in organic based electrolytes (glycerol based electrolyte) an electrolyte solution containing (0.5, 1, 1.5 and 2 wt.% NH4F) then added water (2 and 5Wt.% H2O) to (0.5wt.% NH4F) only with 15V. The range of anodizing time and potential were between 1-4hr. and 5-40V, where Wt.% represent weight percentage. Scanning electron microscopy (SEM), Atomic force microscopy (AFM) and (XRD) X-Ray diffraction were employed to characterize the morphology and structure of the obtained Titania templates, optical interferometer (Fizeau frings) method to tubes length measurement.

Biographie de l'auteur

Haidar H.Hamdan Al-Eqaby and Marwa Abdul Muhsien Hassan Al-Janabi received the B.Sc degree in physics from Al-Mustansiriyah university, Iraq in 2007 and M.Sc degree in Department of Physics from Baghdad and Al-Mustansiriyah university, Iraq in 2012 and 2010 respectively.

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Autres éditions populaires du même titre

9783659540837: Fabrication of TiO2 Nanotubes Using Electrochemical Anodization: Metal oxide nanotube

Edition présentée

ISBN 10 :  3659540838 ISBN 13 :  9783659540837
Editeur : LAP LAMBERT Academic Publishing, 2014
Couverture souple