High Resolution NMR in the Solid State : Fundamentals of CP/MAS

Memory, J. D., Stejskal, E. O.

ISBN 10: 0195073800 / ISBN 13: 9780195073805

Edité par Oxford University Press, Incorporated, 1994

A propos de cet article

Former library book; may include library markings. Used book that is in clean, average condition without any missing pages. N° de réf. du vendeur GRP93284107

Détails bibliographiques

Titre : High Resolution NMR in the Solid State : ...

Éditeur : Oxford University Press, Incorporated

Date d'édition : 1994

Reliure : Couverture rigide

Etat : Good

Edition : 1st Edition.

A propos de ce titre

Synopsis :

This text was developed from a course for physical chemistry and chemical physics students using cross-polarization (CP) magic angle spinning (MAS) NMR in their laboratory assignments. The book provides students with the details of the CP/MAS experiment as it is used to obtain rare-spin, high-resolution NMR spectra. The design of the CP/MAS experiments and the interpretation of spectra and relaxation measurements require an understanding of the interplay of several fundamental physical interactions not normally encountered in solution NMR. The student can observe the way interacting spin systems behave in the solid state, and have a quantum mechanically rigorous understanding of solid-state spin phenomena. The text will have the added benefit of serving as a self-study resource for students seeking to learn the underlying principles of laboratory experiments using the technique. The history of NMR is also treated, and the instrumentation of the spectrometer and probe are discussed.

Présentation de l'éditeur:

Nuclear Magnetic Resonance is used by both physicists and chemists to determine the structure and behaviour of solid materials. This book, for advanced undergraduates and graduate students in both disciplines, aims to provide substantial information on a particular spectroscopic experiment, the cross-polarization (CP) magic angle spinning (MAS) experiment, which is used to obtain rare-spin, high resolution NMR spectra. The text explains clearly the underlying principles of NMR, as well as those involved in this particular experimental method. It can be used by either the student or the working spectroscopist needing to learn the underlying principles of the laboratory experiments they are using.