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Edité par Springer-Verlag Berlin and Heidelberg GmbH & Co. KG, Berlin, 2012
ISBN 10 : 3642264255 ISBN 13 : 9783642264252
Langue: anglais
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Ajouter au panierPaperback. Etat : new. Paperback. Thisbookistalkingabouthowtousesupercriticalwater(SCW)torapidlyproduce micro- and nano-particles of metal oxides, inorganic salts, metals and organics. Itcoversbasicprinciples,experimentalmethodologiesandreactors,particlep- duction,characterizationsandapplicationsaswellastherecentadvanceme nt. Fine particlescanbeproducedbybothchemicalandphysicalprecipitationofproducts from SCW. They can be used as catalysts, materials in ceramics and electronic devices andcompositematerials. Particlesareeasilyproduced continuouslyina owreactorinshortreactiontimes(0. 4s?2min)butcanalsobesynthesizedin batchreactorsforlongreactiontimes(e. g. ,12h). Theycanbeeasilystudiedin-situ microscopically(optical/IR/Raman/SR-XRD)inanopticalmicro-reactor,diamond anvilcell. Thesize,sizedistribution,crystalgrowth&structure,andmorphologyof particlescanbecontrolledbychangingtheconcentrationsofstatingmaterials,pH, pressures,temperatures,heating&coolingrates,organicmodi cations,reducingor oxidizingatmospheres, owratesandreactiontimes. Thisisthe rstbooktosystematicallyintroduceusingSCWforproductionof neparticles. Itisanidealreferencebookforengineers,researchersandgraduate studentsinmaterialscienceandengineering. vii Acknowledgments I would like to thank Drs.T. Ogi & T. Minowa (Biomass Technology Research Center,NationalInstituteofAdvancedIndustrialScienceandTechnology,Japan), and Profs. K. Arai, H. Inomata, R. L. Smith Jr. and T. Adschiri (Chemical Engineering,TohokuUniversity,Japan),whoinitiallyintroducedthehydrothermal andsupercritical uidsareastomewhenIworkedinJapanfrom1996to1999. Thanks are also due to Profs. J. A. Kozinski, R. I. L. Guthrie (Materials Engineering,McGillUniversity,Canada)andI. S. Butler(Chemistry,McGill)for theirguidanceinmyworkonhydrothermalprocessduringmyworkinCanadafrom 1999to2007. Profs. W. Bassett (Geological Sciences, Cornell University) and D. Baker (Earth&PlanetarySciences,McGill)forinstructionsregardingDAC,Dr. I-Ming Chou(U. S. GeologicalSurvey)forusefuldiscussionsofthepressurecalculation procedure. Drs. M. Watanabe and T. Sato (Research Center of Supercritical Fluid Technology, Tohoku University, Japan) for discussions about the experimental set-upofthebatchand owreactors. Drs. S. Xu,H. Assaaoudi,R. HashaikehandA. Sobhy,whoworkedwithmeat McGillinCanada. ix Contents 1 Introduction.1 1. 1 Background .1 1. 2 RapidExpansionofSupercriticalSolution(RESS)Process .4 1.3 SupercriticalAntisolvent(SAS)Process .4 1. 4 OtherPhysicalProcesses .5 1. 5 SupercriticalWaterProcess .5 References.8 2 Supercritical Water Process.11 2. 1 Introduction .11 2. 2 BatchReactor .15 2. 3 FlowReactor.18 2. 4 DiamondAnvilCell(DAC).20 References.25 3 Metal Oxides Synthesis.29 3. 1 Introduction .29 3. 2 Boehmite(AlOOH) .30 3. 3 Ferrites.31 3. 4 Phosphor(YAG) .32 3. 5 LiCoO /LiMn O .33 2 2 4 3. 6 Ce Zr O (x =0?1).33 1?x x 2 3. 7 PotassiumHexatitanate,PotassiumNiobateandTitania .35 3. 8 ZincOxide.38 3. 9 Nickel,Nickel/CobaltOxide. This book details progress in use of supercritical water (SCW) to synthesize nano- and micro- oxides, inorganic salts and metal particles, and shows how polymer/biomass particles can be produced by the precipitation of solutes from SCW. Shipping may be from multiple locations in the US or from the UK, depending on stock availability.
Edité par Springer-Verlag Berlin and Heidelberg GmbH & Co. KG, Berlin, 2010
ISBN 10 : 3642129862 ISBN 13 : 9783642129865
Langue: anglais
Vendeur : Grand Eagle Retail, Bensenville, IL, Etats-Unis
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Autre deviseQuantité disponible : 1 disponible(s)
Ajouter au panierHardcover. Etat : new. Hardcover. Thisbookistalkingabouthowtousesupercriticalwater(SCW)torapidlyproduce micro- and nano-particles of metal oxides, inorganic salts, metals and organics. Itcoversbasicprinciples,experimentalmethodologiesandreactors,particlep- duction,characterizationsandapplicationsaswellastherecentadvanceme nt. Fine particlescanbeproducedbybothchemicalandphysicalprecipitationofproducts from SCW. They can be used as catalysts, materials in ceramics and electronic devices andcompositematerials. Particlesareeasilyproduced continuouslyina owreactorinshortreactiontimes(0. 4s?2min)butcanalsobesynthesizedin batchreactorsforlongreactiontimes(e. g. ,12h). Theycanbeeasilystudiedin-situ microscopically(optical/IR/Raman/SR-XRD)inanopticalmicro-reactor,diamond anvilcell. Thesize,sizedistribution,crystalgrowth&structure,andmorphologyof particlescanbecontrolledbychangingtheconcentrationsofstatingmaterials,pH, pressures,temperatures,heating&coolingrates,organicmodi cations,reducingor oxidizingatmospheres, owratesandreactiontimes. Thisisthe rstbooktosystematicallyintroduceusingSCWforproductionof neparticles. Itisanidealreferencebookforengineers,researchersandgraduate studentsinmaterialscienceandengineering. vii Acknowledgments I would like to thank Drs.T. Ogi & T. Minowa (Biomass Technology Research Center,NationalInstituteofAdvancedIndustrialScienceandTechnology,Japan), and Profs. K. Arai, H. Inomata, R. L. Smith Jr. and T. Adschiri (Chemical Engineering,TohokuUniversity,Japan),whoinitiallyintroducedthehydrothermal andsupercritical uidsareastomewhenIworkedinJapanfrom1996to1999. Thanks are also due to Profs. J. A. Kozinski, R. I. L. Guthrie (Materials Engineering,McGillUniversity,Canada)andI. S. Butler(Chemistry,McGill)for theirguidanceinmyworkonhydrothermalprocessduringmyworkinCanadafrom 1999to2007. Profs. W. Bassett (Geological Sciences, Cornell University) and D. Baker (Earth&PlanetarySciences,McGill)forinstructionsregardingDAC,Dr. I-Ming Chou(U. S. GeologicalSurvey)forusefuldiscussionsofthepressurecalculation procedure. Drs. M. Watanabe and T. Sato (Research Center of Supercritical Fluid Technology, Tohoku University, Japan) for discussions about the experimental set-upofthebatchand owreactors. Drs. S. Xu,H. Assaaoudi,R. HashaikehandA. Sobhy,whoworkedwithmeat McGillinCanada. ix Contents 1 Introduction.1 1. 1 Background .1 1. 2 RapidExpansionofSupercriticalSolution(RESS)Process .4 1.3 SupercriticalAntisolvent(SAS)Process .4 1. 4 OtherPhysicalProcesses .5 1. 5 SupercriticalWaterProcess .5 References.8 2 Supercritical Water Process.11 2. 1 Introduction .11 2. 2 BatchReactor .15 2. 3 FlowReactor.18 2. 4 DiamondAnvilCell(DAC).20 References.25 3 Metal Oxides Synthesis.29 3. 1 Introduction .29 3. 2 Boehmite(AlOOH) .30 3. 3 Ferrites.31 3. 4 Phosphor(YAG) .32 3. 5 LiCoO /LiMn O .33 2 2 4 3. 6 Ce Zr O (x =0?1).33 1?x x 2 3. 7 PotassiumHexatitanate,PotassiumNiobateandTitania .35 3. 8 ZincOxide.38 3. 9 Nickel,Nickel/CobaltOxide. This book details progress in use of supercritical water (SCW) to synthesize nano- and micro- oxides, inorganic salts and metal particles, and shows how polymer/biomass particles can be produced by the precipitation of solutes from SCW. Shipping may be from multiple locations in the US or from the UK, depending on stock availability.
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Edité par Springer Berlin Heidelberg, 2012
ISBN 10 : 3642264255 ISBN 13 : 9783642264252
Langue: anglais
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Edité par Springer Berlin Heidelberg, 2010
ISBN 10 : 3642129862 ISBN 13 : 9783642129865
Langue: anglais
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Edité par Springer Berlin Heidelberg, Springer Berlin Heidelberg Aug 2010, 2010
ISBN 10 : 3642129862 ISBN 13 : 9783642129865
Langue: anglais
Vendeur : buchversandmimpf2000, Emtmannsberg, BAYE, Allemagne
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Ajouter au panierBuch. Etat : Neu. Neuware -Profs. W. Bassett (Geological Sciences, Cornell University) and D. Baker (Earth&PlanetarySciences,McGill)forinstructionsregardingDAC,Dr. I-Ming Chou(U. S. GeologicalSurvey)forusefuldiscussionsofthepressurecalculation procedure. Drs. M. Watanabe and T. Sato (Research Center of Supercritical Fluid Technology, Tohoku University, Japan) for discussions about the experimental set-upofthebatchand owreactors. Drs. S. Xu,H. Assaaoudi,R. HashaikehandA. Sobhy,whoworkedwithmeat McGillinCanada. ix Contents 1 Introduction. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 1. 1 Background . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 1. 2 RapidExpansionofSupercriticalSolution(RESS)Process . . . 4 1. 3 SupercriticalAntisolvent(SAS)Process . . . . . . . . . . . . . 4 1. 4 OtherPhysicalProcesses . . . . . . . . . . . . . . . . . . . . . 5 1. 5 SupercriticalWaterProcess . . . . . . . . . . . . . . . . . . . . 5 References. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8 2 Supercritical Water Process. . . . . . . . . . . . . . . . . . . . . . 11 2. 1 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 2. 2 BatchReactor . . . . . . . . . . . . . . . . . . . . . . . . . . . 15 2. 3 FlowReactor. . . . . . . . . . . . . . . . . . . . . . . . . . . . 18 2. 4 DiamondAnvilCell(DAC). . . . . . . . . . . . . . . . . . . . 20 References. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25 3 Metal Oxides Synthesis. . . . . . . . . . . . . . . . . . . . . . . . . 29 3. 1 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29 3. 2 Boehmite(AlOOH) . . . . . . . . . . . . . . . . . . . . . . . . 30 3. 3 Ferrites. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31 3. 4 Phosphor(YAG) . . . . . . . . . . . . . . . . . . . . . . . . . . 32 3. 5 LiCoO /LiMn O . . . . . . . . . . . . . . . . . . . . . . . . . 33 2 2 4 3. 6 Ce Zr O (x =0 1). . . . . . . . . . . . . . . . . . . . . . 33 1 x x 2 3Springer Verlag GmbH, Tiergartenstr. 17, 69121 Heidelberg 120 pp. Englisch.
Edité par Springer Berlin Heidelberg, 2012
ISBN 10 : 3642264255 ISBN 13 : 9783642264252
Langue: anglais
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Ajouter au panierTaschenbuch. Etat : Neu. Druck auf Anfrage Neuware - Printed after ordering - This book shows how to use supercritical water (SCW) to synthesize nano- andmicro- oxides, inorganic salts and metal particles and its recentadvancement. Also polymer/biomass particles can be produced by using themethod of precipitation of solutes from SCW. The particles can be used ascatalysts for biomass conversions, materials in ceramics & electronic devicesand composite materials. Particles are easily produced continuously ina flow reactor in short reaction times or synthesized in a batch reactor in long reaction times. Besides the synthesis process, the book also present studies of the properties of these materials. The size, size distribution, crystal growth & structure, and morphology of particles produced by supercritical water can be controlled by the feed concentrations, pH, pressures, temperatures, heating & cooling rates, organic modifications, reducing or oxidizing atmospheres, flow rates and reaction times.
Edité par Springer Berlin Heidelberg, 2010
ISBN 10 : 3642129862 ISBN 13 : 9783642129865
Langue: anglais
Vendeur : AHA-BUCH GmbH, Einbeck, Allemagne
EUR 106,99
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Ajouter au panierBuch. Etat : Neu. Druck auf Anfrage Neuware - Printed after ordering - This book shows how to use supercritical water (SCW) to synthesize nano- andmicro- oxides, inorganic salts and metal particles and its recentadvancement. Also polymer/biomass particles can be produced by using themethod of precipitation of solutes from SCW. The particles can be used ascatalysts for biomass conversions, materials in ceramics & electronic devicesand composite materials. Particles are easily produced continuously ina flow reactor in short reaction times or synthesized in a batch reactor in long reaction times. Besides the synthesis process, the book also present studies of the properties of these materials. The size, size distribution, crystal growth & structure, and morphology of particles produced by supercritical water can be controlled by the feed concentrations, pH, pressures, temperatures, heating & cooling rates, organic modifications, reducing or oxidizing atmospheres, flow rates and reaction times.
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Ajouter au panierPaperback. Etat : Brand New. 2010 edition. 120 pages. 9.20x6.10x0.30 inches. In Stock.
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ISBN 10 : 3642129862 ISBN 13 : 9783642129865
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Edité par Springer-Verlag Berlin and Heidelberg GmbH & Co. KG, Berlin, 2012
ISBN 10 : 3642264255 ISBN 13 : 9783642264252
Langue: anglais
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Ajouter au panierPaperback. Etat : new. Paperback. Thisbookistalkingabouthowtousesupercriticalwater(SCW)torapidlyproduce micro- and nano-particles of metal oxides, inorganic salts, metals and organics. Itcoversbasicprinciples,experimentalmethodologiesandreactors,particlep- duction,characterizationsandapplicationsaswellastherecentadvanceme nt. Fine particlescanbeproducedbybothchemicalandphysicalprecipitationofproducts from SCW. They can be used as catalysts, materials in ceramics and electronic devices andcompositematerials. Particlesareeasilyproduced continuouslyina owreactorinshortreactiontimes(0. 4s?2min)butcanalsobesynthesizedin batchreactorsforlongreactiontimes(e. g. ,12h). Theycanbeeasilystudiedin-situ microscopically(optical/IR/Raman/SR-XRD)inanopticalmicro-reactor,diamond anvilcell. Thesize,sizedistribution,crystalgrowth&structure,andmorphologyof particlescanbecontrolledbychangingtheconcentrationsofstatingmaterials,pH, pressures,temperatures,heating&coolingrates,organicmodi cations,reducingor oxidizingatmospheres, owratesandreactiontimes. Thisisthe rstbooktosystematicallyintroduceusingSCWforproductionof neparticles. Itisanidealreferencebookforengineers,researchersandgraduate studentsinmaterialscienceandengineering. vii Acknowledgments I would like to thank Drs.T. Ogi & T. Minowa (Biomass Technology Research Center,NationalInstituteofAdvancedIndustrialScienceandTechnology,Japan), and Profs. K. Arai, H. Inomata, R. L. Smith Jr. and T. Adschiri (Chemical Engineering,TohokuUniversity,Japan),whoinitiallyintroducedthehydrothermal andsupercritical uidsareastomewhenIworkedinJapanfrom1996to1999. Thanks are also due to Profs. J. A. Kozinski, R. I. L. Guthrie (Materials Engineering,McGillUniversity,Canada)andI. S. Butler(Chemistry,McGill)for theirguidanceinmyworkonhydrothermalprocessduringmyworkinCanadafrom 1999to2007. Profs. W. Bassett (Geological Sciences, Cornell University) and D. Baker (Earth&PlanetarySciences,McGill)forinstructionsregardingDAC,Dr. I-Ming Chou(U. S. GeologicalSurvey)forusefuldiscussionsofthepressurecalculation procedure. Drs. M. Watanabe and T. Sato (Research Center of Supercritical Fluid Technology, Tohoku University, Japan) for discussions about the experimental set-upofthebatchand owreactors. Drs. S. Xu,H. Assaaoudi,R. HashaikehandA. Sobhy,whoworkedwithmeat McGillinCanada. ix Contents 1 Introduction.1 1. 1 Background .1 1. 2 RapidExpansionofSupercriticalSolution(RESS)Process .4 1.3 SupercriticalAntisolvent(SAS)Process .4 1. 4 OtherPhysicalProcesses .5 1. 5 SupercriticalWaterProcess .5 References.8 2 Supercritical Water Process.11 2. 1 Introduction .11 2. 2 BatchReactor .15 2. 3 FlowReactor.18 2. 4 DiamondAnvilCell(DAC).20 References.25 3 Metal Oxides Synthesis.29 3. 1 Introduction .29 3. 2 Boehmite(AlOOH) .30 3. 3 Ferrites.31 3. 4 Phosphor(YAG) .32 3. 5 LiCoO /LiMn O .33 2 2 4 3. 6 Ce Zr O (x =0?1).33 1?x x 2 3. 7 PotassiumHexatitanate,PotassiumNiobateandTitania .35 3. 8 ZincOxide.38 3. 9 Nickel,Nickel/CobaltOxide. This book details progress in use of supercritical water (SCW) to synthesize nano- and micro- oxides, inorganic salts and metal particles, and shows how polymer/biomass particles can be produced by the precipitation of solutes from SCW. Shipping may be from our Sydney, NSW warehouse or from our UK or US warehouse, depending on stock availability.
Edité par Springer-Verlag Berlin and Heidelberg GmbH & Co. KG, Berlin, 2010
ISBN 10 : 3642129862 ISBN 13 : 9783642129865
Langue: anglais
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Ajouter au panierHardcover. Etat : new. Hardcover. Thisbookistalkingabouthowtousesupercriticalwater(SCW)torapidlyproduce micro- and nano-particles of metal oxides, inorganic salts, metals and organics. Itcoversbasicprinciples,experimentalmethodologiesandreactors,particlep- duction,characterizationsandapplicationsaswellastherecentadvanceme nt. Fine particlescanbeproducedbybothchemicalandphysicalprecipitationofproducts from SCW. They can be used as catalysts, materials in ceramics and electronic devices andcompositematerials. Particlesareeasilyproduced continuouslyina owreactorinshortreactiontimes(0. 4s?2min)butcanalsobesynthesizedin batchreactorsforlongreactiontimes(e. g. ,12h). Theycanbeeasilystudiedin-situ microscopically(optical/IR/Raman/SR-XRD)inanopticalmicro-reactor,diamond anvilcell. Thesize,sizedistribution,crystalgrowth&structure,andmorphologyof particlescanbecontrolledbychangingtheconcentrationsofstatingmaterials,pH, pressures,temperatures,heating&coolingrates,organicmodi cations,reducingor oxidizingatmospheres, owratesandreactiontimes. Thisisthe rstbooktosystematicallyintroduceusingSCWforproductionof neparticles. Itisanidealreferencebookforengineers,researchersandgraduate studentsinmaterialscienceandengineering. vii Acknowledgments I would like to thank Drs.T. Ogi & T. Minowa (Biomass Technology Research Center,NationalInstituteofAdvancedIndustrialScienceandTechnology,Japan), and Profs. K. Arai, H. Inomata, R. L. Smith Jr. and T. Adschiri (Chemical Engineering,TohokuUniversity,Japan),whoinitiallyintroducedthehydrothermal andsupercritical uidsareastomewhenIworkedinJapanfrom1996to1999. Thanks are also due to Profs. J. A. Kozinski, R. I. L. Guthrie (Materials Engineering,McGillUniversity,Canada)andI. S. Butler(Chemistry,McGill)for theirguidanceinmyworkonhydrothermalprocessduringmyworkinCanadafrom 1999to2007. Profs. W. Bassett (Geological Sciences, Cornell University) and D. Baker (Earth&PlanetarySciences,McGill)forinstructionsregardingDAC,Dr. I-Ming Chou(U. S. GeologicalSurvey)forusefuldiscussionsofthepressurecalculation procedure. Drs. M. Watanabe and T. Sato (Research Center of Supercritical Fluid Technology, Tohoku University, Japan) for discussions about the experimental set-upofthebatchand owreactors. Drs. S. Xu,H. Assaaoudi,R. HashaikehandA. Sobhy,whoworkedwithmeat McGillinCanada. ix Contents 1 Introduction.1 1. 1 Background .1 1. 2 RapidExpansionofSupercriticalSolution(RESS)Process .4 1.3 SupercriticalAntisolvent(SAS)Process .4 1. 4 OtherPhysicalProcesses .5 1. 5 SupercriticalWaterProcess .5 References.8 2 Supercritical Water Process.11 2. 1 Introduction .11 2. 2 BatchReactor .15 2. 3 FlowReactor.18 2. 4 DiamondAnvilCell(DAC).20 References.25 3 Metal Oxides Synthesis.29 3. 1 Introduction .29 3. 2 Boehmite(AlOOH) .30 3. 3 Ferrites.31 3. 4 Phosphor(YAG) .32 3. 5 LiCoO /LiMn O .33 2 2 4 3. 6 Ce Zr O (x =0?1).33 1?x x 2 3. 7 PotassiumHexatitanate,PotassiumNiobateandTitania .35 3. 8 ZincOxide.38 3. 9 Nickel,Nickel/CobaltOxide. This book details progress in use of supercritical water (SCW) to synthesize nano- and micro- oxides, inorganic salts and metal particles, and shows how polymer/biomass particles can be produced by the precipitation of solutes from SCW. Shipping may be from our Sydney, NSW warehouse or from our UK or US warehouse, depending on stock availability.
Edité par Springer Berlin Heidelberg Aug 2010, 2010
ISBN 10 : 3642129862 ISBN 13 : 9783642129865
Langue: anglais
Vendeur : BuchWeltWeit Ludwig Meier e.K., Bergisch Gladbach, Allemagne
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Ajouter au panierBuch. Etat : Neu. This item is printed on demand - it takes 3-4 days longer - Neuware -This book shows how to use supercritical water (SCW) to synthesize nano- andmicro- oxides, inorganic salts and metal particles and its recentadvancement. Also polymer/biomass particles can be produced by using themethod of precipitation of solutes from SCW. The particles can be used ascatalysts for biomass conversions, materials in ceramics & electronic devicesand composite materials. Particles are easily produced continuously ina flow reactor in short reaction times or synthesized in a batch reactor in long reaction times. Besides the synthesis process, the book also present studies of the properties of these materials. The size, size distribution, crystal growth & structure, and morphology of particles produced by supercritical water can be controlled by the feed concentrations, pH, pressures, temperatures, heating & cooling rates, organic modifications, reducing or oxidizing atmospheres, flow rates and reaction times. 120 pp. Englisch.
Edité par Springer Berlin Heidelberg Okt 2012, 2012
ISBN 10 : 3642264255 ISBN 13 : 9783642264252
Langue: anglais
Vendeur : BuchWeltWeit Ludwig Meier e.K., Bergisch Gladbach, Allemagne
EUR 106,99
Autre deviseQuantité disponible : 2 disponible(s)
Ajouter au panierTaschenbuch. Etat : Neu. This item is printed on demand - it takes 3-4 days longer - Neuware -This book shows how to use supercritical water (SCW) to synthesize nano- andmicro- oxides, inorganic salts and metal particles and its recentadvancement. Also polymer/biomass particles can be produced by using themethod of precipitation of solutes from SCW. The particles can be used ascatalysts for biomass conversions, materials in ceramics & electronic devicesand composite materials. Particles are easily produced continuously ina flow reactor in short reaction times or synthesized in a batch reactor in long reaction times. Besides the synthesis process, the book also present studies of the properties of these materials. The size, size distribution, crystal growth & structure, and morphology of particles produced by supercritical water can be controlled by the feed concentrations, pH, pressures, temperatures, heating & cooling rates, organic modifications, reducing or oxidizing atmospheres, flow rates and reaction times. 120 pp. Englisch.
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Edité par Springer Berlin Heidelberg, Springer Berlin Heidelberg Okt 2012, 2012
ISBN 10 : 3642264255 ISBN 13 : 9783642264252
Langue: anglais
Vendeur : buchversandmimpf2000, Emtmannsberg, BAYE, Allemagne
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Ajouter au panierTaschenbuch. Etat : Neu. This item is printed on demand - Print on Demand Titel. Neuware -Profs. W. Bassett (Geological Sciences, Cornell University) and D. Baker (Earth&PlanetarySciences,McGill)forinstructionsregardingDAC,Dr. I-Ming Chou(U. S. GeologicalSurvey)forusefuldiscussionsofthepressurecalculation procedure. Drs. M. Watanabe and T. Sato (Research Center of Supercritical Fluid Technology, Tohoku University, Japan) for discussions about the experimental set-upofthebatchand owreactors. Drs. S. Xu,H. Assaaoudi,R. HashaikehandA. Sobhy,whoworkedwithmeat McGillinCanada. ix Contents 1 Introduction. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 1. 1 Background . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 1. 2 RapidExpansionofSupercriticalSolution(RESS)Process . . . 4 1. 3 SupercriticalAntisolvent(SAS)Process . . . . . . . . . . . . . 4 1. 4 OtherPhysicalProcesses . . . . . . . . . . . . . . . . . . . . . 5 1. 5 SupercriticalWaterProcess . . . . . . . . . . . . . . . . . . . . 5 References. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8 2 Supercritical Water Process. . . . . . . . . . . . . . . . . . . . . . 11 2. 1 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 2. 2 BatchReactor . . . . . . . . . . . . . . . . . . . . . . . . . . . 15 2. 3 FlowReactor. . . . . . . . . . . . . . . . . . . . . . . . . . . . 18 2. 4 DiamondAnvilCell(DAC). . . . . . . . . . . . . . . . . . . . 20 References. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25 3 Metal Oxides Synthesis. . . . . . . . . . . . . . . . . . . . . . . . . 29 3. 1 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29 3. 2 Boehmite(AlOOH) . . . . . . . . . . . . . . . . . . . . . . . . 30 3. 3 Ferrites. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31 3. 4 Phosphor(YAG) . . . . . . . . . . . . . . . . . . . . . . . . . . 32 3. 5 LiCoO /LiMn O . . . . . . . . . . . . . . . . . . . . . . . . . 33 2 2 4 3. 6 Ce Zr O (x =0 1). . . . . . . . . . . . . . . . . . . . . . 33 1 x x 2 3Springer Verlag GmbH, Tiergartenstr. 17, 69121 Heidelberg 120 pp. Englisch.